HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → 2,7-Dipivaloyloxyfluorenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 2,7-Dihydroxylfluorenone | HCID 136365795 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2,7-Dipivaloyloxyfluorenone | HCID 70377329 | — |
Reaction Steps
2.1 g (0.01 mole) of 2,7-dihydroxyfluorenone and 2.5 g (0.025 mole) of pivaloyl chloride were warmed to 50° C. in 6 mls of pyridine in a drying tube attached for 2 hrs. The solvent was removed via rotary evaporator and H2O was added. The crystals were filtered and air dried. Recrystallized from ethanol; 3 g (79%); M.P.~174°-175° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801610 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-713894ec76ce4592b3178b97674e4c20 |
| Source note | uspto-grants-1989_01 |