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HRID2292199

反应详情

EQUATION

反应方程式

HRID 2292199 的结构方程式

REACTANTS

反应物

2
结构：O=C(c1ccccc1)c1ccc(O)cc1
HCID14347

4-Hydroxybenzophenone

C13H10O2

结构：O=C(Cl)C1CCCCC1
HCID75938

Cyclohexanecarbonyl chloride

C7H11ClO

PRODUCTS

生成物

1
结构：O=C(c1ccccc1)c1ccc(OC(=O)C2CCCCC2)cc1
HCID849299

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccncc1
溶剂HCID1049

Pyridine

C5H5N

PROCEDURE

实验过程

The title compound was prepared from 6.0 g of 4-hydroxybenzophenone, 6.0 ml of cyclohexanecarbonyl chloride, pyridine (70 ml). Recrystallized from ethyl acetate-ethanol-water; M.P.~111°-112° C.

WORKUP

后处理

  1. customRecrystallized from ethyl acetate-ethanol-water