Acetyl chloride → 4-Acetoxybenzophenone

HRID 2292202Notes

Reaction equation

HRID 2292202 reaction equation
[OH:1][C:2]1[CH:15]=[CH:14][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:4][CH:3]=1.[C:16](Cl)(=[O:18])[CH3:17]>N1C=CC=CC=1>[C:16]([O:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)=[O:7])=[CH:14][CH:15]=1)(=[O:18])[CH3:17]

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 143474-Hydroxybenzophenone

Product 1

HCID 6077164-Acetoxybenzophenone

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

The title compound was prepared from 4-hydroxybenzophenone and acetyl chloride in pyridine and recrystallized from ethanol (M.P.~82°-83.5° C.). See J. Chem. Soc., 2867 (1927).

Workup

  1. customrecrystallized from ethanol (M.P.~82°-83.5° C.)

Sources & evidence

ORD record
ord-80e2c05592114f5183d9a607929b33f3
Source dataset
uspto-grants-1989_01
Patent number
US04801610

Reaction notes

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