Chlorodimethylsilane → HCID 13529575, compound

HRID 2292243Notes

Reaction equation

HRID 2292243 reaction equation
[CH3:1][C:2](=[C:5]([CH3:8])[CH2:6][CH3:7])[CH2:3][CH3:4].[CH3:9][SiH:10]([CH3:12])[Cl:11].[Al+3].[Cl-].[Cl-].[Cl-]>>[CH2:3]([C:2]([Si:10]([CH3:12])([CH3:9])[Cl:11])([CH3:1])[CH:5]([CH2:6][CH3:7])[CH3:8])[CH3:4]

Participants

4

Reactant 3

HCID 66108ChlorodimethylsilaneHCID 881513-Hexene, 3,4-dimethyl-HCID 6451240Aluminum(III) Chloride

Product 1

HCID 13529575HCID 13529575, compound

Procedure

According to Example 2, 200 mg of 3,4-dimethylhex-3-ene, 0.2 ml (1.8 mmol) of dimethylchlorosilane and 50 mg (0.37 mmol) of AlCl3 are reacted and the product is worked up. This gives 180 mg (50% of theory) of colourless liquid of boiling point=95°-97° C./0.26 mbar.

Workup

  1. customare reacted

Sources & evidence

ORD record
ord-93729467ea684b449325c9140e4c4b85
Source dataset
uspto-grants-1989_01
Patent number
US04801719

Reaction notes

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