Allyl bromide → HCID 641694, compound

HRID 2292255Notes

Reaction equation

[F:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.[CH2:9](Br)[CH:10]=[CH2:11]>>[F:1][C:2]1[CH:3]=[C:4]([O:8][CH2:11][CH:10]=[CH2:9])[CH:5]=[CH:6][CH:7]=1

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 97433-Fluorophenol

Product 1

HCID 641694HCID 641694, compound

Procedure

3-fluoro-phenol was reacted with allyl bromide to form 3-fluoro-allyloxy-benzene with a refractive index of nD23 =1.4985 which was reacted with nitric acid to obtain 2-allyloxy-4-fluoro-nitro-benzene with a refractive index of nD23 =1.5432 which was reacted as in Example 1 to obtain 0-(4-nitro-3-allyloxy-phenyl)-hydroxylamine melting at 94°-95° C.

Sources & evidence

ORD record: ord-bc47adfdf8104f65ab50ea17e7e00745
Source dataset: uspto-grants-1989_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04801717

Reaction notes

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