Ethanol → HCID 136342839, compound

Participants

Reaction Steps

Hydroxylamine hydrochloride (2 g) was dissolved in 20 ml of water and added to 2,5-diallyl-3,6-dihydroxybenzaldehyde (2 g). Enough ethanol was added to completely solubilise the aldehyde. The mixture was heated on a steam bath for ten minutes until TLC showed the reaction to be complete. The water and ethanol were evaporated and the solid recrystallised from ethanol/water, to give a beige solid, m.p. 241°-243° C.

Provenance & Evidence