HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-(3,4-Dihydroxybenzoyl)-2-oxo-1-imidazolidinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-[3,4-Bis(acetyloxy)benzoyl]-2-oxo-1-imidazolidinecarboxamide | HCID 14390896 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | 3-(3,4-Dihydroxybenzoyl)-2-oxo-1-imidazolidinecarboxamide | HCID 21277177 | — |
Reaction Steps
To a suspension of 6.2 g (0.017 mol) of 3-[3,4-bis(acetyloxy)benzoyl]-2-oxo-1-imidazolidinecarboxamide in 50 ml of a 1:1 mixture of ethanol/water was added dropwise 2.1 ml of ammonia. After stirring for 10 minutes, a clear solution formed from which 3-(3,4-dihydroxybenzoyl)-2-oxo-1-imidazolidinecarboxamide began to crystallize after 15 minutes, yielding 3.8 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801705 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-4b990338ecb94998a18f47026256e91b |
| Source note | uspto-grants-1989_01 |