HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 21277154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21277209 | HCID 21277209 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21277154 | HCID 21277154 | — |
Reaction Steps
To a solution of 3.4 g (17.5 mmol) of 1-(3,4-dihydroxyphenyl)-2-imidazolidinone in 10 ml of ethyl acetate was added 7.6 g (70 mmol) of chlorotrimethylsilane, and subsequently 7.0 g (70 mmol) of triethylamine. After stirring overnight at room temperature, the precipitate was filtered off under nitrogen and the filtrate evaporated to dryness in vacuo; yield: 7.14 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801705 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-bc821350ceea4b678071e6ac31de2bb8 |
| Source note | uspto-grants-1989_01 |