HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 2-(4'-Bromophenyl)-5-n-octyl-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 2-Octylpropane-1,3-diol | HCID 316062 | — |
| Product | 2-(4'-Bromophenyl)-5-n-octyl-1,3-dioxane | HCID 12924967 | — |
Reaction Steps
Quantities: compound from Example 9 (48.3 g, 0.26 mol), 4-bromobenzaldehyde (46.5 g, 0.25 mol) and 4-toluenesulphonic acid (150 mg). The experimental procedure was as described in Example 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-9d49a6bf75de440f9b9b88a06cf01cf3 |
| Source note | uspto-grants-1997_11 |