HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 2-(4'-Bromophenyl)-5-n-nonyl-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 2-Nonylpropane-1,3-diol | HCID 3969744 | — |
| Product | 2-(4'-Bromophenyl)-5-n-nonyl-1,3-dioxane | HCID 21477964 | — |
Reaction Steps
Quantities: compound from Example 10 (40.5 g, 0.2 mol), 4-bromobenzaldehyde (37 g, 0.2 mol) and 4-toluenesulphonic acid (150 mg). The experimental procedure was as described in Example 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-07737e58cf4f41fcafbfebd7cfc6d9aa |
| Source note | uspto-grants-1997_11 |