HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triisopropyl borate → (2,3-Difluoro-4-heptylphenyl)boronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | HCID 21477955 | HCID 21477955 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | (2,3-Difluoro-4-heptylphenyl)boronic acid | HCID 22290093 | — |
Reaction Steps
Quantities: compound from Example 24 (31.4 g, 0.15 mol), n-butyllithium (15 cm3, 10.0M in hexanes, 0.15 mol) and triisopropyl borate (56.4 g, 0.3 mol). The experimental procedure was as described in Example 28.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-f518f3efc238455caeccb85245991f1a |
| Source note | uspto-grants-1997_11 |