HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triisopropyl borate → (2,3-Difluoro-4-octylphenyl)boronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | 2,3-Difluoro-1-octylbenzene | HCID 14495629 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | (2,3-Difluoro-4-octylphenyl)boronic acid | HCID 19359093 | — |
Reaction Steps
Quantities: compound from Example 25 (31 g, 0.14 mol), n-butyllithium (14 cm3, 10.0M in hexanes, 0.14 mol) and triisopropyl borate (52.7 g, 0.28 mol). The experimental procedure was as described in Example 28.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-4212ef43f77344fc8c7fc4e4b52fbf45 |
| Source note | uspto-grants-1997_11 |