HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triisopropyl borate → (4-Decyl-2,3-difluorophenyl)boronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triisopropyl borate | HCID 21531 | — |
| Reactant | 1-Decyl-2,3-difluorobenzene | HCID 21477945 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | (4-Decyl-2,3-difluorophenyl)boronic acid | HCID 19359100 | — |
Reaction Steps
Quantities: compound from Example 27 (26.7 g, 105 mmol), n-butyllithium (11 cm3, 10.0M in hexanes, 0.11 mol) and triisopropyl borate (39.5 g, 0.21 mol). The experimental procedure was as described in Example 28.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-cefa6fa38fc448fb9da0b4f41d76270c |
| Source note | uspto-grants-1997_11 |