Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2292430Generated: November 1, 2026

Triisopropyl borate → [2,3-Difluoro-4-(heptyloxy)phenyl]boronic acid

https://huagongshe.com/reaction/2292430

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriisopropyl borateHCID 21531—
Reactant1,2-Difluoro-3-(heptyloxy)benzeneHCID 21477947—
ReactantButyllithiumHCID 178418339—
Product[2,3-Difluoro-4-(heptyloxy)phenyl]boronic acidHCID 21477961—

Reaction Steps

Quantities: n-butyllithium (20 cm3, 10.0M in hexanes, 0.2 mol), compound from Example 40 (45.5 g, 0.2 mol) and triisopropyl borate (74.4 g, 0.4 mol). The experimental procedure was as described in Example 28.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05683623
Source datasetuspto-grants-1997_11
ORD IDord-af23ae372b474ac0926e3d034badfe5f
Source noteuspto-grants-1997_11