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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2292431Generated: November 1, 2026

Triisopropyl borate → (2,3-Difluoro-4-(octyloxy)phenyl)boronic acid

https://huagongshe.com/reaction/2292431

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriisopropyl borateHCID 21531—
Reactant1,2-Difluoro-3-(octyloxy)benzeneHCID 10562497—
ReactantButyllithiumHCID 178418339—
Product(2,3-Difluoro-4-(octyloxy)phenyl)boronic acidHCID 10850744—

Reaction Steps

Quantities: n-butyllithium (10 cm3, 10.0M in hexanes, 0.1 mol), compound from Example 41 (23.4 g, 0.1 mol) and triisopropyl borate (37.6 g, 0.2 mol). The experimental procedure was as described in Example 28.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05683623
Source datasetuspto-grants-1997_11
ORD IDord-c80776576d6a468b88619fb615e40f3f
Source noteuspto-grants-1997_11