HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 2-(2',3'-Difluorophenyl)-5-n-nonyl-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 2,3-Difluorobenzaldehyde | HCID 137664 | — |
| Reactant | 2-Nonylpropane-1,3-diol | HCID 3969744 | — |
| Product | 2-(2',3'-Difluorophenyl)-5-n-nonyl-1,3-dioxane | HCID 21477941 | — |
Reaction Steps
Quantities: compound from Example 10 (31.4 g, 0.155 mol), 2,3-difluorobenzaldehyde (21.5 g, 0.15 mol) and 4-toluenesulphonic acid (100 mg). The experimental procedure was as described in Example 114.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683623 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-66902cd48da8445ab4a02dd2d7ce15b4 |
| Source note | uspto-grants-1997_11 |