HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53678991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54236856 | HCID 54236856 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 53678991 | HCID 53678991 | — |
Reaction Steps
By the method of Example 1, Step E, 10.92 grams (0.046 mole) of 2,5-dichloro-3-methoxyphenylacetic acid and 40 mL of thionyl chloride were reacted in approximately 200 mL of carbon tetrachloride, yielding 11.92 grams of 2,5-dichloro-3-methoxyphenylacetyl chloride as a black oil. The IR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05683966 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-f62eebf94ee144259190e981daa70af2 |
| Source note | uspto-grants-1997_11 |