Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2292630Generated: November 1, 2026

Sodium ethanethiolate → HCID 53892591, compound

https://huagongshe.com/reaction/2292630

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium ethanethiolateHCID 4459711—
ReactantHCID 53939961HCID 53939961—
SolventWaterHCID 962—
SolventDimethylformamideHCID 6228—
SolventDichloromethaneHCID 6344—
ProductHCID 53892591HCID 53892591—

Reaction Steps

Combine 2-(4-methoxybenzoyl)-4-benzenesulfonylimino-4H-chromene (1 mmol) and sodium thioethoxide (2 mmol) in dimethylformamide (5 mL). Stir for 48 hours. Dilute the reaction mixture with water and dichloromethane. Separate the organic layer, dry over MgSO4, filter, and evaporate in vacuo. Chromatograph on silica gel to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05684017
Source datasetuspto-grants-1997_11
ORD IDord-7de88091c92744358dfa2352aa4edfc6
Source noteuspto-grants-1997_11