HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethanethiolate → HCID 53892591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethanethiolate | HCID 4459711 | — |
| Reactant | HCID 53939961 | HCID 53939961 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53892591 | HCID 53892591 | — |
Reaction Steps
Combine 2-(4-methoxybenzoyl)-4-benzenesulfonylimino-4H-chromene (1 mmol) and sodium thioethoxide (2 mmol) in dimethylformamide (5 mL). Stir for 48 hours. Dilute the reaction mixture with water and dichloromethane. Separate the organic layer, dry over MgSO4, filter, and evaporate in vacuo. Chromatograph on silica gel to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05684017 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-7de88091c92744358dfa2352aa4edfc6 |
| Source note | uspto-grants-1997_11 |