Fumarate → HCID 70196425, compound

HRID 2292641Notes

Reaction equation

HRID 2292641 reaction equation
[CH:1]1([CH2:9][CH2:10][C:11](O)=O)[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH2:2]1.[O:14]1[C:20]2[CH:21]=[CH:22][C:23]([N:25]3[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]3)=[CH:24][C:19]=2[O:18][CH:17]=[CH:16][CH2:15]1.C([O-])(=O)/C=C/C([O-])=O>>[CH:1]1([CH2:9][CH2:10][CH2:11][N:28]2[CH2:29][CH2:30][N:25]([C:23]3[CH:22]=[CH:21][C:20]4[O:14][CH2:15][CH:16]=[CH:17][O:18][C:19]=4[CH:24]=3)[CH2:26][CH2:27]2)[C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[CH2:2]1

Participants

4

Reactant 3

HCID 5460307FumarateHCID 10397308HCID 10397308, compoundHCID 70197230HCID 70197230, compound

Product 1

HCID 70196425HCID 70196425, compound

Procedure

Prepared as described in Example 9, starting from 3-(benzocyclobutan-1-yl)propionic acid and 4-(benzo-1,5-dioxepin-7-yl)piperazine. The fumarate of the title compound melts at 168°-170° C. (ethanol).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-d1f7f48242664317aec0838268a4f7e8
Source dataset
uspto-grants-1997_11
Patent number
US05684020

Reaction notes

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