HCID 15839404, compound → HCID 18918750, compound
Reaction equation
[CH2:1]1[C:5]2=[CH:6][C:7]([C:9](O)=O)=[CH:8][C:4]2=[CH:3][S:2]1.[CH3:12][O:13][C:14]1[C:15]([N:23]2[CH2:28][CH2:27][NH:26][CH2:25][CH2:24]2)=[CH:16][C:17]2[O:21][CH2:20][CH2:19][C:18]=2[CH:22]=1>>[CH2:1]1[C:5]2=[CH:6][C:7]([CH2:9][N:26]3[CH2:27][CH2:28][N:23]([C:15]4[C:14]([O:13][CH3:12])=[CH:22][C:18]5[CH2:19][CH2:20][O:21][C:17]=5[CH:16]=4)[CH2:24][CH2:25]3)=[CH:8][C:4]2=[CH:3][S:2]1Participants
3
Procedure
Prepared as described in Example 9, starting from (cyclopenta[c]thien-5-yl)carboxylic acid (Preparation 7) and 4-(2,3-dihydro-5-methoxybenzofuran-6-yl)piperazine. The title compound melts at 156°-158° C.
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-66d8e5c29b8e4b968a4787e8021c431a
- Source dataset
- uspto-grants-1997_11
- Patent number
- US05684020
Reaction notes
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