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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2292698Generated: October 31, 2026

4-Benzyloxybenzyl chloride → HCID 21479375, compound

https://huagongshe.com/reaction/2292698

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Benzyloxybenzyl chlorideHCID 70042—
Reactant6-Chloropiperonyl chlorideHCID 90113—
ReactantEthyl 5-(phenylmethoxy)-1H-indole-2-carboxylateHCID 95721—
ProductHCID 21479375HCID 21479375—

Reaction Steps

Following the procedure of Example 1(a)-1(d), except substituting ethyl indole-2-carboxylate for ethyl 5-benzyloxyindole-2-carboxylate in step (a) and 4-benzyloxybenzyl chloride for 6-chloropiperonyl chloride in step (c), the title compound was prepared (39% overall). mp 193°-194° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05684032
Source datasetuspto-grants-1997_11
ORD IDord-920e5aa810bc481ebb8fa64e4de047c6
Source noteuspto-grants-1997_11