HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxyphenylpyruvic Acid → (+-)-3-(4-Hydroxyphenyl)lactic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxyphenylpyruvic Acid | HCID 979 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (+-)-3-(4-Hydroxyphenyl)lactic acid | HCID 9378 | 99.9% |
Reaction Steps
10 g of 3-(4-hydroxyphenyl)pyruvic acid were dissolved in 50 ml of methanol, and 0.05 g of platinum oxide was added thereto. The mixture was stirred at 25° C. under atmospheric pressure for 6 hours in a hydrogen stream. After completion of the reaction, the catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure to give 10.1 g of 3-(4-hydroxyphenyl)lactic acid as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05684186 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-2e9aaf13be724adba0ad8022282f92a2 |
| Source note | uspto-grants-1997_11 |