N,N,N-trimethylglycinium → HCID 21903092, compound

HRID 2292865Notes

Reaction equation

[CH3:1][N:2]([CH3:4])[CH3:3].C[N+](CC(O)=O)(C)C.Cl.C[NH+](C)C.[Cl:18][CH2:19][C:20]([OH:22])=[O:21]>>[Cl:18][CH2:19][C:20]([O-:22])=[O:21].[CH3:1][NH+:2]([CH3:4])[CH3:3]

Participants

Reactant 4

HCID 248N,N,N-trimethylglycinium

HCID 300Chloroacetic Acid

HCID 1146Trimethylamine

HCID 22606969HCID 22606969, compound

Product 1

HCID 21903092HCID 21903092, compound

Procedure

maintaining the reaction solution from step (1) at pH 7.5-10, as necessary, by addition of a molar excess of liquid trimethylamine, to effect the formation of betaine and trimethyl ammonium hydrochloride until substantially all of the monochloroacetic acid has been reacted, leaving a residual amount of trimethylammoniumchloroacetate in the reaction solution;

Workup

customhas been reacted

Sources & evidence

ORD record: ord-bc1343f353a648b5a9a2f92446700a9f
Source dataset: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05684191

Reaction notes

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