Epichlorohydrin → HCID 21480166, compound

HRID 2292880Notes

Reaction equation

HRID 2292880 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[CH:3]=1.[CH2:9]([CH:11]1[O:13][CH2:12]1)Cl>>[CH2:9]([N:1]([CH2:9][CH:11]1[O:13][CH2:12]1)[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([CH3:8])[CH:3]=1)[CH:11]1[O:13][CH2:12]1

Participants

3

Reactant 2

HCID 7835EpichlorohydrinHCID 7934m-Toluidine2×

Product 1

HCID 21480166HCID 21480166, compoundYield 100%

Procedure

1 mole of N,N-bisglycidyl-m-toluidine was prepared from 4.8 moles of m-toluidine and 2 moles of epichlorohydrin. The excess m-toluidine was required to produce the oxirane ring and was filtered off as the hydrochloride after completion of the reaction.

Workup

  1. customto produce the oxirane ring
  2. filtrationwas filtered off as the hydrochloride
  3. customafter completion of the reaction

Sources & evidence

ORD record
ord-4b335c76630c4513b3103f5fd0d19360
Source dataset
uspto-grants-1997_11
Patent number
US05684202

Reaction notes

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