HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21475499, compound → HCID 21475503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21475499 | HCID 21475499 | — |
| Reactant | 2-Nitro-N~1~-(prop-2-en-1-yl)benzene-1,4-diamine | HCID 23500036 | — |
| Product | HCID 21475503 | HCID 21475503 | — |
Reaction Steps
Synthesis as for compound 1, but with 4-fluoro-3-nitro-N,N-bis-(2,3-dihydroxypropyl)-aminobenzene instead of 4-fluoro-3-nitroaminobenzene. Working up: the reaction mixture was concentrated and the dark oil was dissolved in ethanol. Compound (3) was then precipitated with HCl gas in the form of the hydrochloride. Yellow crystals, melting point 154°-158° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05685881 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-5b22937ee964497f8ae222e96df0dda0 |
| Source note | uspto-grants-1997_11 |