HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178451298, compound → HCID 178512834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178451298 | HCID 178451298 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178512834 | HCID 178512834 | — |
Reaction Steps
67.5 g of Z-Arg-Gly-OtBu are suspended in 800 ml of absolute tetrahydrofuran and refluxed for 2 hours. The mixture is then concentrated and the residue is triturated with methyl tert.-butyl ether. The precipitate is filtered off with suction and dried. Yield 54.2 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686421 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-f0c17134e97f4176bedc90a0e8297c98 |
| Source note | uspto-grants-1997_11 |