HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (-)- → (S)-1-methyl-1,2,3,4-tetrahydroisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Reactant | HCID 10964792 | HCID 10964792 | — |
| Product | (S)-1-methyl-1,2,3,4-tetrahydroisoquinoline | HCID 11205845 | — |
Reaction Steps
In accordance with the same procedures as in Preparation 1-2, except that 25.6 ml of (S)-1-phenylethyl-amine(0.20M) and 34.8 g of α-chloro-α-(methylthio)-acetyl chloride(0.22M) were used as starting materials, 8.8 g of the title compound was obtained in oil form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686458 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-250520ab047e40b7aa4769c7a87addae |
| Source note | uspto-grants-1997_11 |