Acetyl chloride → HCID 13143595, compound

HRID 2293136Notes

Reaction equation

[CH3:1][CH:2]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)[CH2:3][NH2:4].[C:11](Cl)(=O)[CH3:12]>>[CH3:11][CH:12]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:2]([CH3:1])[CH2:3][NH:4]1

Participants

Reactant 2

HCID 6367Acetyl chloride

HCID 113982-Phenylpropylamine

Product 1

HCID 13143595HCID 13143595, compound

Procedure

In accordance with the same procedures as in Preparation 1-1, except that 14.5 ml of β-methylphenethyl-amine(0.1M) and 7.8 ml of acetyl chloride(0.11M) were used as starting materials, 6.6 g of the title compound was prepared.

Workup

customIn accordance with the same procedures as in Preparation 1-1

Sources & evidence

ORD record: ord-5d1c49fd72b840bdbbd6010ec0ca1c11
Source dataset: uspto-grants-1997_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05686458

Reaction notes

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