HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-[(2-methylbenzoyl)amino]benzoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-[(2-methylbenzoyl)amino]benzoic Acid | HCID 11615814 | — |
| Product | 4-[(2-methylbenzoyl)amino]benzoyl Chloride | HCID 10707441 | — |
Reaction Steps
A mixture of 10.3 g of 4-[(2-methylbenzoyl)amino]benzoic acid and 32 ml of thionyl chloride is refluxed for 1.5 hours. The solution is concentrated under vacuum. Toluene is added and the solvent removed under vacuum. Toluene is added and the mixture chilled and filtered to give a yellow solid, m.p. 135°-141° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686445 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-00331801023d4ef8885e8d5b42cf9a9a |
| Source note | uspto-grants-1997_11 |