HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzaldehyde → HCID 69954567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzaldehyde | HCID 66042 | — |
| Reactant | L-Proline | HCID 145742 | — |
| Reactant | HCID 18361637 | HCID 18361637 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 69954567 | HCID 69954567 | — |
Reaction Steps
7.B)g) (3aRS,4SR,8aRS,8bSR)-4-(2-Cyclohexylmethyl-1,3-dioxo-decahydro-pyrrolo[3,4-a]pyrrolizin-4-yl)-benzonitrile was prepared analogously to Example 4.B)g) from 4-cyano-benzaldehyde, L-proline and N-cyclohexylmethylmaleimide. Colourless crystals. M.p.: 119°-122° C. (ethyl acetate/hexane). ISP-MS: 378.4 ([M+H]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686459 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-4ff1a3cc803c4e789398bdf6827419d7 |
| Source note | uspto-grants-1997_11 |