HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzaldehyde → HCID 69954989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzaldehyde | HCID 66042 | — |
| Reactant | L-Thioproline | HCID 93176 | — |
| Reactant | HCID 708821 | HCID 708821 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69954989 | HCID 69954989 | — |
Reaction Steps
7.B)h) (5RS,5aRS,8aSR,8bRS)-4-[7-(Benzo[1,3]dioxol-5-ylmethyl)-6,8-dioxo-octahydro-pyrrolo[3',4':3,4]pyrrolo[1,2-c]thiazol-5-yl]-benzonitrile was prepared analogously to Example 4.B)g) from 4-cyano-benzaldehyde, L-thioproline and N-piperonylmaleimide. Colourless needles. M.p.: 142°-143° C. (methanol). ISP-MS: 434.2 ([M+H]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686459 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-f59af2b39a29452c85132cb59c4c04ca |
| Source note | uspto-grants-1997_11 |