HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131720308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131720309 | HCID 131720309 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 131720308 | HCID 131720308 | — |
Reaction Steps
Following the procedure described in Example 120, the coupling of N-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl]-L-proline hydrochloride (250 mg, 0.69 mmol) and 1-methyl-3-phenylpropylamine (0.34 mL, 2.1 mmol) provided, after treatment with HCl in Et2O, 40 mg of the hydrochloride salt of L-proline, 1-[2-(3,4,5-trimethoxyphenyl)-2-oxoethyl] 1-methyl-3-phenylpropylamide as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686424 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-58491882a25f486e9c2f3aa8528c5a86 |
| Source note | uspto-grants-1997_11 |