HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Phenylbenzoyl chloride → HCID 22879064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| Reactant | HCID 22873003 | HCID 22873003 | — |
| Product | HCID 22879064 | HCID 22879064 | 83% |
Reaction Steps
Using the procedure described in Example 7, treatment of 1-[2-(S)-amino-4-methylpentyl]-L-proline 4-phenylbutylamide (112 mg) with 4-biphenyl carbonyl chloride (95 mg) provided 128 mg (83%) of the title compound. The 1H NMR and Mass spectrum analysis of this compound was consistent with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686469 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-8889b6c1c9a744bc9620237b1683143d |
| Source note | uspto-grants-1997_11 |