HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenecarbonyl chloride → HCID 22879066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenecarbonyl chloride | HCID 70146 | — |
| Reactant | HCID 22873003 | HCID 22873003 | — |
| Product | HCID 22879066 | HCID 22879066 | 42% |
Reaction Steps
Using the procedure described in Example 7, treatment of 1-[2-(S)-amino-4-methylpentyl]-L-proline 4-phenylbutylamide (120 mg) with 1-naphthoyl chloride (71 uL) provided 66 mg (42%) of the title compound. The 1H NMR and Mass spectrum analysis of this compound was consistent with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686469 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-d94c9198f8d94e97b1722df2380248e7 |
| Source note | uspto-grants-1997_11 |