HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 9868506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 67940172 | HCID 67940172 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 9868506 | HCID 9868506 | — |
Reaction Steps
The compound (43) (0.305 g) was dissolved in a mixed solvent (6 ml) consisting of acetic acid, THF and water (2:1:1) and kept at 50° C. for 14 hours. The resultant mixture was worked up with the conventional procedure and the obtained crude product was subjected to silicagel column chromatography to give the titled compound (44). Yield: 0.213 g (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686487 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-ca3c66d09a5b4ba197512f745a9e1ffc |
| Source note | uspto-grants-1997_11 |