HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 59910718, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 86746860 | HCID 86746860 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59910718 | HCID 59910718 | — |
Reaction Steps
The compound (45) (0.311 g) was dissolved in a mixed solvent (5 ml) consisting of acetic acid, THF and water (2:1:1) and kept at 50° C. for 3 hours. The resultant mixture was worked up with the conventional procedure and the residue was subjected to silicagel column chromatography to give the titled compound (46). Yield: 0.156 g (66%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686487 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-b366df9f3a5b468883a49e84ea7a4e96 |
| Source note | uspto-grants-1997_11 |