HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86746863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 86746861 | HCID 86746861 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86746863 | HCID 86746863 | — |
Reaction Steps
The compound (56) (0.514 g) was dissolved in a mixed solvent (30 ml) consisting of acetic acid, THF and water (4:2:1) and the solution was kept overnight at the room temperature. The resultant mixture was worked up with the conventional procedure and the obtained crude product was subjected to silicagel column chromatography to give the titled compound (46). Yield: 0.272 g (61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686487 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-77dd542e43f244bb8c55bddf48199f93 |
| Source note | uspto-grants-1997_11 |