HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86746863, compound → HCID 59910751, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86746863 | HCID 86746863 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 59910751 | HCID 59910751 | — |
Reaction Steps
A solution of the compound (46) (0.272 g) in acetic acid (10 ml) was treated with zinc (3.5 g) added in portions at the room temperature for 2.5 hours. The resultant mixture was worked up with the conventional procedure and the residue was subjected to silicagel column chromatography to give the titled compound (57). Yield: 0.177 g (81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686487 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-d5f9d58613a840598fb1db67b536aa96 |
| Source note | uspto-grants-1997_11 |