HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromotoluene → HCID 67720907, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromotoluene | HCID 7805 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 54042416 | HCID 54042416 | — |
| Product | HCID 67720907 | HCID 67720907 | — |
Reaction Steps
1.5 g (5 mmoles) of 2-[3-(5,6,7,8-tetrahydro-5,5, 8,8-tetramethyl-2-naphthyl)-allyl]-1,3-dioxane, 850 mg (5 mmoles) of 4-bromotoluene, 25 mg (0.1 mmole) of Pd (OAc)2, 55 mg (0.2 mmole) of P(C6H5)3 and 1.4 g (10 mmoles) of potassium carbonate are heated at 180° C. for 2 hours under passage of nitrogen.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686586 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-965250a7d3a846f2b3f281b8075e1bb0 |
| Source note | uspto-grants-1997_11 |