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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2293795Generated: October 31, 2026

Potassium ethanethioate → HCID 57142678, compound

https://huagongshe.com/reaction/2293795

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium ethanethioateHCID 23670855—
ReactantHCID 57286434HCID 57286434—
ProductHCID 57142678HCID 5714267843.2%

Reaction Steps

Methyl (2RS,3S)-3-tert-butoxycarbonylamino-2-acetylthio-3-(2-fluorophenyl) propionate may be prepared in a similar manner to that described in Example 1G, but starting with 30 g of methyl (2R,3S)-3-tert-butoxycarbonylamino-2-tosyloxy-3-(2-fluorophenyl)propionate and 17.2 g of potassium thioacetate. 9.8 g of methyl (2RS,3S)-3-tert-butoxycarbonylamino-2-acetylthio-3-phenylpropionate are thus obtained in the form of a red oil which is used without further purification in the subsequent syntheses.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05686622
Source datasetuspto-grants-1997_11
ORD IDord-27c65cdbc44140ceb075bf473a42a494
Source noteuspto-grants-1997_11