HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium ethanethioate → HCID 57142678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium ethanethioate | HCID 23670855 | — |
| Reactant | HCID 57286434 | HCID 57286434 | — |
| Product | HCID 57142678 | HCID 57142678 | 43.2% |
Reaction Steps
Methyl (2RS,3S)-3-tert-butoxycarbonylamino-2-acetylthio-3-(2-fluorophenyl) propionate may be prepared in a similar manner to that described in Example 1G, but starting with 30 g of methyl (2R,3S)-3-tert-butoxycarbonylamino-2-tosyloxy-3-(2-fluorophenyl)propionate and 17.2 g of potassium thioacetate. 9.8 g of methyl (2RS,3S)-3-tert-butoxycarbonylamino-2-acetylthio-3-phenylpropionate are thus obtained in the form of a red oil which is used without further purification in the subsequent syntheses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05686622 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-27c65cdbc44140ceb075bf473a42a494 |
| Source note | uspto-grants-1997_11 |