HRID2293814

反应详情

EQUATION

反应方程式

HRID 2293814 的结构方程式

PROCEDURE

实验过程

338.58 g (1 mol) of erucic acid (purity 95%) were ozonized in analogy to Example 1 and then hydrogenation was carried out. The hydrogenation solution obtained in this way contained nonanal and tridecanealdehyde acid and was divided by distillation. For oxidation, the corresponding aldehyde fraction was employed and was oxidized at 14 bar in analogy to Example 1. 185 g of tridecanedioic acid per cycle were obtained with a purity of 95%.

WORKUP

后处理

  1. customThe hydrogenation solution obtained in this way
  2. distillationwas divided by distillation