Propanal → HCID 12297951, compound

HRID 229383Notes

Reaction equation

[N+:1]([C:4]1[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=1[NH2:6])([O-])=O.[CH:11](=O)[CH2:12][CH3:13]>>[CH2:12]([CH:11]1[NH:6][C:5]2[C:4](=[CH:10][CH:9]=[CH:8][CH:7]=2)[N:1]2[CH:10]=[CH:4][CH:5]=[C:7]12)[CH3:13]

Participants

Reactant 2

HCID 527Propanal

HCID 69462-Nitroaniline

Product 1

HCID 12297951HCID 12297951, compound

Procedure

The title compound was prepared from 2-nitro aniline according to the sequence of Example 1 and 2, and the resulting oil treated with proprionaldehyde according to the procedure of Example 3 to yield a light orange oil, which was used in the next step without further characterization.

Workup

customto yield a light orange oil, which

Sources & evidence

ORD record: ord-1e71cc694fca4ce7bef0cf0bdf3af4f7
Source dataset: uspto-grants-2009_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07563793B2

Reaction notes

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