Propanal → HCID 69064194, compound

HRID 229384Notes

Reaction equation

HRID 229384 reaction equation
[CH3:1][C:2]1[C:3]([N+:9]([O-])=O)=[C:4]([CH:6]=[CH:7][CH:8]=1)[NH2:5].[CH:12](=O)[CH2:13][CH3:14]>>[CH2:13]([CH:12]1[NH:9][C:3]2[C:4](=[CH:6][CH:7]=[CH:8][C:2]=2[CH3:1])[N:5]2[CH:1]=[CH:2][CH:8]=[C:7]12)[CH3:14]

Participants

3

Reactant 2

HCID 527PropanalHCID 690383-Methyl-2-nitroaniline

Product 1

HCID 69064194HCID 69064194, compound

Procedure

The title compound was prepared 3-methyl-2-nitro aniline according to the sequence of Examples 1 and 2, and the resulting oil treated with proprionaldehyde according to the procedure of Example 3 to yield a brown solid, mp 65-68° C.

Workup

  1. customto yield a brown solid, mp 65-68° C.

Sources & evidence

ORD record
ord-14ab52a3d53f458cb96c898e8dfdb2d4
Source dataset
uspto-grants-2009_07
Patent number
US07563793B2

Reaction notes

Loading…