Boron Trichloride → HCID 11711102, compound

HRID 229385Notes

Reaction equation

HRID 229385 reaction equation
[CH2:1]([CH:3]1[N:12]([S:13]([C:16]2[CH:21]=[CH:20][C:19]([O:22]C)=[C:18]([CH3:24])[CH:17]=2)(=[O:15])=[O:14])[C:11]2[C:6](=[CH:7][C:8]([O:26]C)=[C:9]([F:25])[CH:10]=2)[N:5]2[CH:28]=[CH:29][CH:30]=[C:4]12)[CH3:2].B(Cl)(Cl)Cl>>[CH2:1]([CH:3]1[N:12]([S:13]([C:16]2[CH:21]=[CH:20][C:19]([OH:22])=[C:18]([CH3:24])[CH:17]=2)(=[O:15])=[O:14])[C:11]2[C:6](=[CH:7][C:8]([OH:26])=[C:9]([F:25])[CH:10]=2)[N:5]2[CH:28]=[CH:29][CH:30]=[C:4]12)[CH3:2]

Participants

3

Reactant 2

HCID 25135Boron TrichlorideHCID 69069087HCID 69069087, compound

Product 1

HCID 11711102HCID 11711102, compound

Procedure

The title compound was prepared from the product of Example 73 following the procedure of Example 5 but using 4 equivalents of boron trichloride to yield light tan crystals, mp 194-196° C.

Workup

  1. customto yield light tan crystals, mp 194-196° C.

Sources & evidence

ORD record
ord-98943873ce144e24ac1e70e6cfe87a88
Source dataset
uspto-grants-2009_07
Patent number
US07563793B2

Reaction notes

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