HCID 131720321, compound → HCID 131720320, compound

Participants

Reaction Steps

Dissolve the product of Example 2 (0.35 g, 0.77 mmol) in EtOAc (6 mL) and purge with N2. Add 10% Pd/C (0.082 g), purge the resulting suspension with H2 and stir under a balloon of H2 for 3 h. Filter the mixture through celite, wash the filter cake with EtOAc and concentrate the filtrate to obtain 0.35 g (100%) of the title compound as a clear oil. MS (EI): 455(M+, 13), 308(31), 217(78), 185(25), 149(52), 129(100).

Provenance & Evidence