HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86749096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 21474127 | HCID 21474127 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Product | HCID 86749096 | HCID 86749096 | 100% |
Reaction Steps
Dissolved 3-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-pyridine (0.95 g, 3.5 mmol) in 50 mL of glacial acetic acid. Added platinum oxide catalyst (0.2 g), and shook on Paar shaker at 59 psi of hydrogen pressure for 24 hours. Filtered, and evaporated filtrate. Crystallized product from ether to give 1.14 g (100% yield) of 3-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-piperidine acetic acid as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05688805 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-5f0189ebd8de4f1680ee90b36156bc7b |
| Source note | uspto-grants-1997_11 |