(3,5-Dimethylphenyl)hydrazine hydrochloride → 4,6-Dimethyltryptamine hydrochloride
Reaction equation
[ClH:1].C[C:3]1C=C2[C:6]([NH:7]C=C2CCN)=[C:5](Br)[CH:4]=1.Cl.[CH3:17][C:18]1[CH:19]=[C:20]([NH:25]N)[CH:21]=[C:22]([CH3:24])[CH:23]=1>>[ClH:1].[CH3:17][C:18]1[CH:23]=[C:22]([CH3:24])[CH:21]=[C:20]2[C:19]=1[C:4]([CH2:5][CH2:6][NH2:7])=[CH:3][NH:25]2Participants
3
Procedure
4,6-Dimethyltryptamine hydrochloride was prepared (1.06 g) as described for 5-methyl-7-bromotryptamine hydrochloride in Example 4, except using 3,5-dimethylphenylhydrazine hydrochloride (7.65 g) as starting material.
Sources & evidence
- ORD record
- ord-05a723a24ab74ed8bdaa881eabc10f8b
- Source dataset
- uspto-grants-1997_11
- Patent number
- US05688807
Reaction notes
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