HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Trifluoroacetate → 4-[2-(1-Benzyl-cyclopropylamino)-1-hydroxy-ethyl]-2-hydroxymethyl-phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Trifluoroacetate | HCID 84468 | — |
| Edukt | 1-Benzylcyclopropylamine | HCID 152923 | — |
| Edukt | Methyl benzyloxy-5-(2-ethoxy-2-hydroxy-acetyl)-benzoate | HCID 68858509 | — |
| Produkt | 4-[2-(1-Benzyl-cyclopropylamino)-1-hydroxy-ethyl]-2-hydroxymethyl-phenol | HCID 11573217 | — |
Reaktionsschritte
Prepared according to general method 5 from 344 mg (1 mmol) methyl 2-benzyloxy-5-(2-ethoxy-2-hydroxy-acetyl)-benzoate and 147 mg (1 mmol) 1-benzyl-cyclopropylamine. Yield: 184 mg (43%, trifluoroacetate); mass spectroscopy: [M+H]+=314.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07563806B2 |
| Quelldatensatz | uspto-grants-2009_07 |
| ORD ID | ord-618792e546dd4c42a8d812714e910d41 |
| Quellennotiz | uspto-grants-2009_07 |