HCID 23433467, compound → HCID 22279055, compound

HRID 2294458Notes

Reaction equation

HRID 2294458 reaction equation
[C:1]([O:5][NH:6][C:7]([C:9]1[C:14]([CH3:15])=[C:13]([N+:16]([O-])=O)[CH:12]=[CH:11][CH:10]=1)=[O:8])([CH3:4])([CH3:3])[CH3:2].C(ONC(C1C=C(C=CC=1)N)=O)(C)(C)C>>[NH2:16][C:13]1[CH:12]=[CH:11][CH:10]=[C:9]([C:7](=[O:8])[NH:6][O:5][C:1]([CH3:2])([CH3:3])[CH3:4])[C:14]=1[CH3:15]

Participants

3

Reactant 2

HCID 23433467HCID 23433467, compoundHCID 23433515HCID 23433515, compound

Product 1

HCID 22279055HCID 22279055, compoundYield 99%

Procedure

This compound was prepared from 6-tert-butyloxycarbamoyl-2-nitrotoluene (4.60 g, 18.2 mmol) in a manner similar to that described for 3-tert-butyloxycarbamoylaniline (EXAMPLE 147), affording 4.00 g (99%) of 2-amino-6-tert-butyloxycarbamoyltoluene as a colorless oil. Data for 2-amino-6-tert-butyloxycarbamoyltoluene:

Sources & evidence

ORD record
ord-0f0f4d7ffb864332aeb9f1a949c8f79f
Source dataset
uspto-grants-1997_11
Patent number
US05688810

Reaction notes

Loading…