4-tert-Butylbenzoyl chloride → Allyl 4-(4-tert-butylbenzoyloxymethyl)benzoate

HRID 2294547Notes

Reaction equation

HRID 2294547 reaction equation
[C:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9](Cl)=[O:10])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[OH:14][CH2:15][C:16]1[CH:27]=[CH:26][C:19]([C:20]([O:22][CH2:23][CH:24]=[CH2:25])=[O:21])=[CH:18][CH:17]=1>>[C:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9]([O:14][CH2:15][C:16]2[CH:17]=[CH:18][C:19]([C:20]([O:22][CH2:23][CH:24]=[CH2:25])=[O:21])=[CH:26][CH:27]=2)=[O:10])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 743724-tert-Butylbenzoyl chlorideHCID 22392687Allyl 4-hydroxymethylbenzoate

Product 1

HCID 21474565Allyl 4-(4-tert-butylbenzoyloxymethyl)benzoate

Procedure

In a manner similar to Example 1(d), by reaction of 2 g (15 mmol) of 4-tert-butylbenzoyl chloride with 2.9 g (15 mmol) of allyl 4-hydroxymethylbenzoate, 4 g (77%) of allyl ester are obtained in the form of a colorless oil.

Workup

  1. customare obtained in the form of a colorless oil

Sources & evidence

ORD record
ord-52bb599eeb4142a29b0bb0b571380d41
Source dataset
uspto-grants-1997_11
Patent number
US05688817

Reaction notes

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